Publicaciones Química Analítica


  1. F.J. Lara, J. Robles, S. Brandt, A. Schütz, B. Gilbert, A. Molina-Díaz, J.F. García-Reyes, J. Franzke (2018). Use of dielectric barrier discharge ionization to minimize matrix effects and expand coverage in pesticide residue analysis by liquid chromatography-mass spectrometry. Analytica Chimica Acta, DOI: [10.1016/j.aca.2018.02.077], ISSN: 0003-2670. Ver
  2. D. Moreno, J. Alcántara, B. Gilbert, M. Beneito, V.M. Cutillas, L. Rajski, A. Molina-Díaz, J.F. García-Reyes (2018). Sensitive detection of neonicotinoid insecticides and other selected pesticides in pollen and nectar using nanoflow liquid chromatography orbitrap tandem mass spectrometry. Journal of AOAC International, 101(2): 367-373, DOI: [10.5740/jaoacint.17-0412].
  3. J.C. Domínguez, B. Gilbert, M. Beneito, A. Molina-Díaz (2018). Renewable chemiluminescence optosensors based on implementation of bead injection principle with multicommutation. Talanta, 182: 267-272, DOI: [10.1016/j.talanta.2018.01.091], ISSN: 0039-9140. Ver
  4. F.J. Lara, B. Gilbert, M. Beneito, A. Molina-Díaz (2018). Multicommuted flow injection analysis using chemiluminescence detection (MCFIA-CL) for olive oil analysis. Food Analytical Methods, 1-11, DOI: [10.1007/s12161-018-1182-5]. Ver
  5. J. Alcántara, D. Moreno, B. Gilbert, A. Molina-Díaz, J.F. García-Reyes (2018). Matrix-effect free multi-residue analysis of veterinary drugs in food samples of animal origin by nanoflow liquid chromatography high resolution mass spectrometry. Food Chemistry, 245: 29-38, DOI: [10.1016/j.foodchem.2017.10.083], ISSN: 0308-8146. Ver
  6. F.J. Lara, M. Beneito, J. Robles, J.F. García-Reyes, B. López, A. Molina-Díaz (2018). Direct olive oil analysis by mass spectrometry: a comparison of different ambient ionization. Talanta, 180: 168-175, DOI: [10.1016/j.talanta.2017.12.027], ISSN: 0039-9140. Ver
  7. R. López, D. Moreno, R. Nortes, J.F. García-Reyes, A. Molina-Díaz, B. Gilbert (2017). Experimental and theoretical determination of pesticide processing factors to model their behaviour during virgin olive oil production. Food Chemistry, 239: 9-16, DOI: [10.1016/j.foodchem.2017.06.086], ISSN: 0308-8146. Ver
  8. D. Moreno, P. Pérez, B. Gilbert, A. Molina-Díaz, J.F. García-Reyes, A.R. Fernández (2017). Evaluation of nanoflow liquid chromatography high resolution mass spectrometry for pesticide residue analysis in food. Journal of Chromatography A, 1512: 78-87, DOI: [10.1016/j.chroma.2017.07.019], ISSN: 0021-9673. Ver
  9. J. Robles, B. Gilbert, J.F. García-Reyes, A. Molina-Díaz (2017). Simultaneous liquid chromatography/mass spectrometry determination of both polar and “multiresidue” pesticides in food using parallel hydrophilic interaction/reversed-phase liquid chromatography and a hybrid sample preparation approach. Journal of Chromatography A, 1517: 108-116, DOI: [10.1016/j.chroma.2017.08.041], ISSN: 0021-9673. Ver
  10. D. Moreno, J. Alcántara, B. Gilbert, J.F. García-Reyes, A. Molina-Díaz (2017). Matrix-effect free quantitative liquid chromatography mass spectrometry analysis in complex matrices using nanoflow liquid chromatography with integrated emitter tip and high dilution factors. Journal of Chormatography A, 1519: 110-120, DOI: [10.1016/j.chroma.2017.09.006], ISSN: 0021-9673. Ver
  11. F.J. Lara, B. Gilbert, J.F. García-Reyes, A. Molina-Díaz (2017). Fast automated determination of total tocopherol content in virgin olive oil using a single multicommu ted luminescent flow method. Food Analytical Methods, 10(7): 2125-2131, DOI: [10.1007/s12161-016-0784-z]. Ver
  12. B. Gilbert, M. Dernovics, D. Moreno, A. Molina-Díaz, J.F. García-Reyes (2017). Detection of over 100 selenium metabolites in selenized yeast by liquid chromatography electrospray time-of-flight mass spectrometry. Journal of Chromatography B, 1060: 84-90, DOI: [10.1016/j.jchromb.2017.06.001], ISSN: 1570-0232. Ver
  13. P. Pérez, F.J. Lara, B. Gilbert, D. Moreno, J.F. García-Reyes, A. Molina-Díaz (2017). Screening of over 600 pesticides, veterinary drugs, food-packaging contaminants, mycotoxins, and other chemicals in food by ultra-high performance liquid chromatography quadrupole time-of-flight mass spectrometry (UHPLC-QTOFMS). Food Analytical Methods, 10(5): 1216-1244, DOI: [10.1007/s12161-016-0678-0]. Ver
  14. J.A. Tuñón, M. Beneito, J. Robles, D.J. Parras, A. Molina-Díaz, A. Sánchez, J.F. García-Reyes (2017). Multiclass profiling of lipids of archaeological interest by ultra-high pressure liquid chromatography atmospheric pressure chemical ionization high resolution mass spectrometry. Microchemical Journal, 132: 49-58, DOI: [10.1016/j.microc.2016.12.023], ISSN: 0026-265X. Ver
  15. P. Berton, N.B. Lana, J.M. Ríos, J.F. García-Reyes, J.C. Altamirano (2016). State-of-the-art of environmentally-friendly sample preparation approaches for determination of PBDEs and metabolites in environmental and biological samples: a critical review. Analytica Chimica Acta, 905: 24-41, DOI: [10.1016/j.aca.2015.11.009], ISSN: 0003-2670. Ver
  16. R. López, B. Gilbert, R. Rojas, J. Robles, N. Ramos, J.F. García-Reyes, A. Molin (2016). Evaluation of processing factors for selected organic contaminants during virgin olive oil production: distribution of BTEXS during olives processing. Food Chemistry, 199: 273-279, DOI: [10.1016/j.foodchem.2015.11.132], ISSN: 0308-8146. Ver
  17. P. Pérez, F.J. Lara, J.F. García-Reyes, B. Gilbert, M. Trojanowicz, A. Molina-Díaz (2016). A feasibility study of UHPLC-HRMS accurate-mass screening methods for multiclass testing of organic contaminants in food. Talanta, 160: 704–712, DOI: [10.1016/j.talanta.2016.08.002], ISSN: 0039-9140. Ver
  18. R. López, R. Nortes, J. Robles, D. Moreno, B. Gilbert, J.F. García-Reyes, A. Molina-Díaz (2016). Evaluation of different cleanup sorbents for multiresidue pesticideanalysis in fatty vegetable matrices by liquid chromatography tandemmass spectrometry. Journal of Chromatography A, 1456:  89–104, DOI: [10.1016/j.chroma.2016.06.019], ISSN: 0021-9673. Ver
  19. R. Nortes, J. Robles, R. López, A. Vass, A. Molina-Díaz, J.F. García-Reyes (2016). Determination of polar pesticides in olive oil and olives by hydrophilic interaction liquid chromatography coupled to tandem mass spectrometry and high resolution mass spectrometry. Talanta, 158: 222–228, DOI: [10.1016/j.talanta.2016.05.058], ISSN: 0039-9140. Ver
  20. F.J. Lara, F.J. Sainz, B. Gilbert, J.F. García-Reyes, A. Molina-Díaz (2016). Multicommuted flow injection method for fast photometric determination of phenolic compounds in commercial virgin olive oil samples. Talanta, 147: 531–536, DOI: [10.1016/j.talanta.2015.10.015], ISSN: 0039-9140. Ver
  21. P. Pérez, F.J. Lara, J.F. García-Reyes, M. Beneito, B. Gilbert, N.R. Martos, A. Molina-Díaz (2016). Determination of over 350 multiclass pesticides in jams by ultra-high performance liquid chromatography time-of-flight mass spectrometry (UHPLC-TOFMS). Food Analytical Methods, 9(7): 1939-1957, DOI: [10.1007/s12161-015-0369-2]. Ver
  22. E. Estévez, M.D.C. Cabrera, J.R. Fernández, A. Molina-Díaz, J. Robles, M.D.P. Palacios (2016). Monitoring priority substances, other organic contaminants and heavy metals in a volcanic aquifer from different sources and hydrological processes. Science of the Total Environment, 551-552, 186-196, DOI: [10.1016/j.scitotenv.2016.01.177], ISSN: 0048-9697. Ver
  23. A. Vass, J. Robles, P. Pérez, B. Gilbert, M. Dernovics, A. Molina-Díaz, J.F. García-Reyes (2016). Study of different HILIC, mixed-mode, and other aqueous normal-phase approaches for the liquid chromatography/mass spectrometry-based determination of challenging polar pesticides. Analytical and Bioanalytical Chemistry, 408(18): 4857-4869, DOI:  [10.1007/s00216-016-9589-6], ISSN: 1618-2650. Ver
  24. D.J. Parras, A. Sanchez, J.A. Tuñón, M.C. Rueda, N. Ramos, J.F. García-Reyes (2015). Sulphur, fats and beeswax in the Iberian rites of the sanctuary of the oppidum of Puente Tablas (Jaén, Spain).  Journal of Archaeologicasl Sciences: Reports, 4: 510-524, DOI: [10.1016/j.jasrep.2015.10.010], ISSN: 2352-409X. Ver
  25. B. Gilbert, J.A. Mendiola, J. Fontecha, V.D. Broek, A.M. Lambertus, L. Sijtsma, A. Cifuentes, M. Herrero, M.E. Ibáñez (2015). Downstream processing of Isochrysis galbana: a step towards microalgal biorefinery. Green Chemistry, 17: 4599-4609, DOI: [10.1039/c5gc01256b]. Ver
  26. A. Bojanowska, G. Kciuk, M. Gumiela, S. Borowiecka, G. Nalecz, A. Koc, J.F. García-Reyes, D.S. Ozbay, M. Trojanowicz (2015). Analytical, toxicological and kinetic investigation of decomposition of the drug diclofenac in waters and wastes using gamma radiation. Environmental Science and Pollution Research, 22(24): 20255-20270, DOI: [10.1007/s11356-015-5236-6]. Ver
  27. J.C. Domínguez, F.J. Lara, J.F. García, A. Molina-Díaz (2015). Screening and confirmation capabilities of liquid chromatography-time-of-flight mass spectrometry for the determination of 200 multiclass sport drugs in urine. Talanta, 134: 74-88, DOI: [10.1016/j.talanta.2014.10.050], ISSN: 0039-9140. Ver
  28. J.C. Domínguez, J.F. García-Reyes, M. Beneito, R. Martínez, E. Martínez, M.L. Del Moral, A. Molina-Díaz (2015). Study of tamoxifen urinary metabolites in rat by ultra-high-performance liquid chromatography time-offlight mass spectrometry. Biomedical Chromatography, 29(8): 1220-1228, DOI: [10.1002/bmc.3411]. Ver
  29. M. Beneito, P. Pérez, A. Molina-Díaz, J.F. García-Reyes (2015). Rapid determination of multiclass fungicides in wine by low-temperature plasma (LTP) ambient ionization mass spectrometry. Analytical Methods, 7: 7345-7351, DOI: [10.1039/c5ay00810g]. Ver
  30. S. Shao, X. Mi, L. Ouerdane, R. Lobinski, J.F. García-Reyes, A. Molina-Díaz, A. Vass, M. Dernovics (2014). Quantification of Se-Methylselenocysteine and Its GAMMA-glutamyl derivative from naturally Se- enriched green bean (Phaseolus vulgaris vulgaris) after HPLC-ESI-TOF-MS and orbitrap MS n –based identification. Food Analytical Methods, 7(5): 1147-1157, DOI: [10.1007/s12161-013-9728-z]. Ver
  31. J. Robles, F.J. Lara, B. Gilbert, J.F. García-Reyes, A. Molina-Díaz (2014). Multi-residue method for the determination of over 400 priority and emerging pollutants in water and wastewater by solid-phase extraction and liquid chromatography-time-of-flight mass spectrometry. Journal of Chromatography A, 1350: 30-43, DOI: [10.1016/j.chroma.2014.05.003], ISSN: 0021-9673. Ver
  32. J.C. Domínguez, J.F. García-Reyes, A. Molina-Díaz (2014). Comparative evaluation of seven different sample treatment approaches for large-scale multiclass sport drug testing in urine by liquid chromatography mass spectrometry. Journal of Chromatography A, 1361: 34-42, DOI: [10.1016/j.chroma.2014.07.090], ISSN: 0021-9673. Ver
  33. B. Gilbert, Z.L. Valencia, V.M. Yufra, J.F. García-Reyes, N. Ramos, A. Molina-Díaz (2014) Determination of polyphenols in commercial extra virgin olive oils from different origins (Mediterranean and South American countries) by liquid chromatography-electrospray time-of-flight mass spectrometry. Food Analytical Methods, 7(9): 1824-1833, DOI: [10.1007/s12161-014-9825-7]. Ver
  34. J. Robles, B. Gilbert, J.F. García-Reyes, A. Molina-Díaz (2014). Monitoring of selected priority and emerging contaminants in the Guadalquivir River and other related surface waters in the province of Jaén, South East Spain. Science of the Total Environment, 479-480, 247-257, DOI: [10.1016/j.scitotenv.2014.01.121], ISSN: 0048-9697. Ver
  35. C. Meyer, S. Müller, B. Gilbert, J. Franzke (2013). Impact of homogeneous and filamentary discharge modes on the efficiency of dielectric barrier discharge ionization mass spectrometry. Analytical And Bioanalytical Chemistry, 405: 4729-4735, DOI: [10.1007/s00216-013-6902-5]. Ver
  36. A. Nemeth, J.F. García-Reyes, J. Kosary, M. Dernovics (2013). The relationship of selenium tolerance and speciation in Lecythidaceae species. Metallomics, 5(12): 1663-1673, DOI: [10.1039/c3mt00140g]. Ver
  37. M. Benassi, J.F. García-Reyes, B. Sprengler (2013). Ambient ion/molecule reactions in low-temperature plasmas (LTP): reative LTP mass spectrometry. Rapid Communications In Mass Spectrometry, 27: 795-804, DOI: [10.1002/rcm.6500]. Ver
  38. E. Pobozy, M. Filaber, A. Koc, J.F. García-Reyes (2013). Application of capillary electrophoretic chips in protein profiling of plant extracts for identification of genetic modifications of maize. Electrophoresis, 34(18): 2740-2753, DOI: [10.1002/elps.201300103]. Ver
  39. J.C. Domínguez, J.F. García-Reyes, R. Martínez, P. Berton, E. Martínez, M.L. del Moral, A. Molina-Díaz (2013). Combined data mining strategy for the systematic identification of sport drug metabolites in urine by liquid chromatography time-of-flight mass spectrometry. Analytica chimica acta, 761: 1-10, DOI: [10.1016/j.aca.2012.11.049], ISSN: 0003-2670. Ver
  40. B. Gilbert, M. Schilling, N. Ahlmann, A. Michels, H. Hayen, A. Molina-Díaz, J.F. García-Reyes, J. Franzke (2013). Ambient diode laser desorption dielectric barrier discharge ionization mass spectrometry of nonvolatile chemicals. Analytical chemistry, 85(6): 3174-3182, DOI: [10.1021/ac303452w]. Ver
  41. J. Robles, B. Gilbert, J.F. García-Reyes, A. Molina-Díaz (2013). Comparative evaluation of liquid-liquid extraction, solid-phase extraction and solid-phase microextraction for the gas chromatography-mass spectrometry determination of multiclass priority organic contaminants in wastewater. Talanta, 117: 382-391, DOI: [10.1016/j.talanta.2013.09.040], ISSN: 0039-9140. Ver
  42. J. Robles, B. Gilbert, J.F. García-Reyes, A. Molina-Díaz (2013). Gas chromatography triple quadrupole mass spectrometry method for monitoring multiclass organic pollutants in Spanish sewage treatment plants effluents. Talanta, 111: 196-205, DOI: [10.1016/j.talanta.2013.03.006], ISSN: 0039-9140. Ver
  43. F.J. Benítez, J.L. Acero, J.F. García-Reyes, F.J. Real, G. Roldán, E. Rodríguez, A. Molina-Díaz (2013). Oxidation of chlorophene by ozonation: kinetics, identification of by-products and reaction pathways. Chemical Engineering Journal, 230: 447-455, DOI: [10.1016/j.cej.2013.06.120], ISSN: 1385-8947. Ver
  44. F.J. Benítez, J.L. Acero, J.F. García-Reyes, F.J. Real, G. Roldán, E. Rodríguez, A. Molina-Díaz (2013). Determination of the reaction rate constants and decomposition mechanisms of ozone with two model emerging contaminants: DEET and nortriptyline. Industrial & engineering Chemical Research, 52: 17064-17073, DOI: [10.1021/ie402916u]. Ver
  45. A. González, J.C. Domínguez, J.F. García-Reyes, P. Rodríguez, G. Centineo, J.I. García, A. Molina-Díaz (2013). Overcoming matrix effects in electrospray: quantitation of -agonists in complex matrices by isotope dilution liquid chromatography mass spectrometry using singly 13C-labeled analogues. Journal of Chromatography A, 1288: 40-47.
  46. J.C. Domínguez, J.F. García-Reyes, R. Martínez, E. Martínez, M.L. Del Moral, A. Molina-Díaz (2013). Detection of main urinary metabolites of 2-agonists clenbuterol, salbutamol and terbutaline by liquid chromatography high resolution mass spectrometry. Journal of Chromatography B, 923-924, 128-135, DOI: [10.1016/j.jchromb.2013.02.008], ISSN: 1570-0232. Ver
  47. C. Indermuhle, M. De Vidales, C. Sáez, J. Robles, P. Cañizares, J.F. García-Reyes, A. Molina-Díaz, C. Comninellis, M. Rodrigo (2013). Degradation of caffeine by conductive diamond electrochemical oxidation. Chemosphere, 93(9): 1720-1725, DOI: [10.1016/j.chemosphere.2013.05.047], ISSN: 0045-6535. Ver
  48. B. Gilbert, H. Geltenpoth, C. Meyer, A.  Michels, H. Hayen, A. Molina-Díaz, J.F. García-Reyes, J. Franzke (2013). Performance of dielectric barrier discharge ionization mass spectrometry for pesticide testing: A comparison with atmospheric pressure chemical ionization and electrospray ionization. Rapid communication in mass spectrometry, 27(3): 419-429, DOI: [10.1002/rcm.6469]. Ver
  49. L. Polgar, B. Kmellar, J.F. García-Reyes, P. Fodor (2012). Comprehensive evaluation of the clean-up step in QUECHERS procedure for the multi-residue determination of pesticides in different vegetable oils using LC-MS/MS. Analytical Methods, 4: 1142-1148, DOI: [10.1039/c2ay05543k]. Ver
  50. L. Abranko, J.F. García-Reyes, A. Molina-Díaz (2012). Systematic bottom-up approach for flavonoid derivative screening in plant material using liquid chromatography high-resolution mass spectrometry. Analytical And Bioanalytical Chemistry, 403(4): 995-1006, DOI: [10.1007/s00216-012-5865-2]. Ver
  51. J. Robles, M.J. Martín, J.F. García-Reyes, P. Cañizares, C. Sáez, M.A. Rodrigo, A. Molina-Díaz (2012). Conductive-diamond electrochemical oxidation of chlorpyrifos in wastewater and identification of its main degradation products by LC-TOFMS. Chemosphere, 89(10): 1169-1176, DOI: [10.1016/j.chemosphere.2012.08.004], ISSN: 0045-6535. Ver
  52. L. Polgár, J.F. García-Reyes, P. Fodor, A. Gyepes, M. Dernovics, L. Abranko, B. Gilbert, A. Molina-Díaz (2012). Retrospective screening of relevant pesticide metabolites in food using liquid chromatography high resolution mass spectrometry and accurate-mass databases of parent molecules and diagnostic fragment ions. Journal of Chromatography A, 1249: 83-91, DOI: [10.1016/j.chroma.2012.05.097], ISSN: 0021-9673. Ver
  53. B. Gilbert, J.F. García-Reyes, C. Meyers, A. Michels, J. Franzke, A. Molina-Díaz, H. Hayen (2012). Simultaneous testing of multiclass organic contaminants in food and environment by liquidchromatography/dielectric barrier discharge ionization-mass spectrometry. Analyst, 137(22): 5403-5410, DOI: [10.1039/c2an35705d]. Ver
  54. P. Berton, J.C. Domínguez, R.G. Wuilloud , B. Sánchez, M. Chaki, A.M. Carreras, R. Valderrama, J.C. Begara-Morales, F.J. Corpas, J.B. Barroso, B. Gilbert, J.F. García-Reyes, A. Molina-Díaz (2012). Determination of nitrotyrosine in Arabidopsis thaliana cell cultures with a mixed-mode solid-phase extraction cleanup followed by liquid chromatography time-of-flight mass spectrometry. Analytical and Bioanalytical Chemistry, 404: 1495-1503, DOI: [10.1007/s00216-012-6220-3]. Ver
  55. P.M. Pérez, B. Gilbert, J.F. García-Reyes, N. Ramos, A. Molina-Díaz (2012). Generic sample treatment method for simultaneous determination of multiclass pe.M. sticides and mycotoxins in wines by liquid chromatography-mass spectrometry. Journal of Chromatography A, 1249: 32-40, DOI: [10.1016/j.chroma.2012.06.020], ISSN: 0021-9673. Ver
  56. A. Koc, A. Cañuelo, J.F. García-Reyes, A. Molina-Díaz, M. Trojanovicz (2012). Low-molecular weight protein profiling of genetically modified maize using fast liquid chromatography electrospray ionization and time-of-flight mass spectrometry. Journal of Separation Science, 35(12): 1447-1461, DOI: [10.1002/jssc.201200109]. Ver
  57. M.J. Martín De Vidales, J. Robles, J.C. Domínguez, P. Cañizares, C. Sáez, A. Molina-Díaz, M.A. Rodrigo (2012). Removal of sulfamethoxazole from waters and wastewaters by conductive-diamond electrochemical oxidation. Journal of Chemical Technology & Biotechnology, 87(10): 1441-1449, DOI: [10.1002/jctb.3766]. Ver
  58. B. Gilbert, L. Jaén, J.F. García-Reyes, M. Villar, L. Polgar, N. Ramos, A. Molina-Díaz (2012). Study on the occurrence of pesticide residues in fruit-based soft drinks from the EU market and morocco using liquid chromatography-mass spectrometry. Food Control, 26(2): 341-346, DOI: [10.1016/j.foodcont.2012.01.025], ISSN: 0956-7135. Ver
  59. B. Gilbert, J.F. García-Reyes, A. Molina-Díaz (2012). Determination of fungicide residues in baby food by liquid chromatography-ion trap tandem mass spectrometry. Food Chemistry, 135(2): 780-786, DOI: [10.1016/j.foodchem.2012.04.059], ISSN: 0308-8146. Ver
  60. E. Estévez, M.C. Cabrera, A. Molina-Díaz, J. Robles, M.P. Palacios (2012). Screening of emerging contaminants and priority substances (2008/105/EC) in a volcanic aquifer (Gran Canaria, Canary Islands, Spain). Science of the total environment, 433: 538-546, DOI: [10.1016/j.scitotenv.2012.06.031], ISSN: 0048-9697. Ver
  61. J.F. García-Reyes, B. Gilbert, A. Agüera, A. Rodríguez, A. Molina-Díaz (2012) The potential of ambient desorption ionization methods combined with high-resolution mass spectrometry for pesticide testing in food. Comprehensive Analytical Chemistry, 58: 339–366, DOI: [10.1016/B978-0-444-53810-9.00004-3].
  62. B. Gilbert, A. Cañuelo, P. Pacheco, E. Martínez, E. Siles, A. Miranda (2012). Tyrosol, a main phenol present in extra virgin olive oil, increases lifespan and stress resistance in Caenorhabditis elegans. Mechanisms of Ageing and Development, 133 (8): 563-574, DOI: [10.1016/j.mad.2012.07.004], ISSN:  0047-6374. Ver



  1. J.F. García-Reyes, B. Gilbert, A. Molina-Díaz (2013). Pesticides: organophospates. In Analysis of Endocrine Disrupting Compounds in Food, pp. 199-218.

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